Characteristic data of activation of crystalline and amorphous OER catalysts with bulk and surface Fe incorporation.
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Description
This electrochemical, X-ray diffraction, and operando X-ray abosorption spectroscopy data characterize and decouple the effects of bulk vs. electrolyte Fe incorporation in crystalline, defective crystalline, and amorphous catalysts derived from the same CoSn(OH)₆ precursor. Electrolyte Fe incorporation equalizes the OER activity across all three structural variants, demonstrating that surface Fe chemistry can dominate initial structural effects on the reconstructed catalyst interface.
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Funding
- Swiss National Science Foundation
- PRIMA PR00P2_193111
References
Journal reference (UNDER REVIEW; Paper in which the electrochemical activation, characterization methods, and structure-activity trends are described in detail.) K. Crossley, J. Grotheer, J. Huang, T.J. Schmidt, E. Fabbri. Advanced Energy and Sustainability Research, (UNDER REVIEW, 2026)